International Journal of Science , Engineering and Management (IJSEM)

Monthly Journal for Science , Engineering and Management

Volume2,November 2017,

Topic : Synthesis and characterization of O,O’-bis-di-α- naphthyl dithiophosphate of lead(II).

Authors:Atiya Syed ||

Abstract:O,O’-bis -di-α-naphthyldithiophosphate of lead(II) corresponding to [(α-C10H7O)2PS2 ]2Pb, has been synthesized by the reaction of PbCl2 in 2:1 molar ratio with sodium salt of O,O’-di-α-naphthyl dithiophosphate in refluxing chloroform. This complex has been characterized by elemental analyses, C, H, S, Pb and further characterization by some spectroscopy analyses, namely, IR and NMR (1H, 13C and 31P) has been carried out. Monomeric nature of this complex has been confirmed and lead atom is four coordinately bonded to two bidentate dithiophosphate ligands leading to a square planar geometry around the lead atom..

Keywords: α-naphthyl, dithiophosphate, lead, phosphorus, sulfur

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DOI: 01.1617/vol4/iss11/pid37289


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Editor-in-Chief

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Dr.Muhammad Ishtiaq,
Mirpur University of
Science & Technology,
Mirpur, Azad Kasmir.

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IMPACT FACTOR: 2.7

ISSN(Online): 2456-1304

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Thomson Reuters ID : q-6288-2016.
ORCiD Research ID : 0000-0001-9540-6799

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ACCEPTANCE RATIO: 25%
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Journal Code : IJSEM
Electronic ISSN : 2456-1304
Impact Factor : 2.7
Frequency : Monthly
Contact : editor@ijsem.org

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